
Thu Aug 16 14:24:54 2001

Sample homogenised #1

Refit _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L' _Si-K' _Si-K" 
Filter Fit Method
Chi-sqd = 1.38     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---        1446 +/-    64
  O -K       ---         ---         785 +/-   143
  Fe-L       ---         ---       10878 +/-   204
  Si-K    0.01528 +/- 0.00028       6407 +/-   117
  Mn-K    0.00886 +/- 0.00116        850 +/-   111
  Fe-K    0.97497 +/- 0.00632      81950 +/-   531
  Mo-L    0.00089 +/- 0.00074        217 +/-   179

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0151   1.529    4.49    2.31    +/- 0.04
  Mn-K    0.0087   1.024    0.89    0.90    +/- 0.12
  Fe-K    0.9628   1.004   94.56   96.68    +/- 0.63
  Mo-L    0.0009   1.310    0.07    0.12    +/- 0.10
  Total                   100.00  100.00            




 

Thu Aug 16 14:29:00 2001

Sample homogenised #2

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Filter Fit Method
Chi-sqd = 2.14     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---        1160 +/-    53
  O -K       ---         ---        1055 +/-    75
  Fe-L       ---         ---       11709 +/-   208
  Si-K    0.01719 +/- 0.00049       7288 +/-   207
  Mn-K    0.00793 +/- 0.00116        769 +/-   112
  Fe-K    0.97331 +/- 0.00634      82700 +/-   539
  Mo-L    0.00157 +/- 0.00075        385 +/-   184

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0169   1.527    5.02    2.59    +/- 0.07
  Mn-K    0.0078   1.025    0.79    0.80    +/- 0.12
  Fe-K    0.9596   1.005   94.07   96.41    +/- 0.63
  Mo-L    0.0016   1.312    0.12    0.20    +/- 0.10
  Total                   100.00  100.00            




 

Thu Aug 16 14:36:38 2001

Sample homogenised #3 Near graphite

Refit _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _C -K' _Fe-L' 
Filter Fit Method
Chi-sqd = 1.41     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---        1149 +/-    50
  O -K       ---         ---         672 +/-   121
  Fe-L       ---         ---       11534 +/-   199
  Si-K    0.01600 +/- 0.00047       6781 +/-   198
  Mn-K    0.00876 +/- 0.00113        850 +/-   109
  Fe-K    0.97264 +/- 0.00627      82629 +/-   533
  Mo-L    0.00259 +/- 0.00075        634 +/-   182

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0158   1.527    4.69    2.41    +/- 0.07
  Mn-K    0.0086   1.024    0.88    0.89    +/- 0.11
  Fe-K    0.9596   1.004   94.24   96.37    +/- 0.62
  Mo-L    0.0026   1.310    0.19    0.34    +/- 0.10
  Total                   100.00  100.00            




 

Thu Aug 16 14:39:44 2001

Sample homogenised #4 Near graphite

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Filter Fit Method
Chi-sqd = 2.33     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         889 +/-    49
  O -K       ---         ---         941 +/-    68
  Fe-L       ---         ---       10800 +/-   188
  Si-K    0.01503 +/- 0.00044       6526 +/-   192
  Mn-K    0.00831 +/- 0.00113        825 +/-   112
  Fe-K    0.97427 +/- 0.00618      84786 +/-   538
  Mo-L    0.00239 +/- 0.00072        598 +/-   180

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0148   1.528    4.41    2.27    +/- 0.07
  Mn-K    0.0082   1.024    0.84    0.84    +/- 0.11
  Fe-K    0.9620   1.004   94.57   96.58    +/- 0.61
  Mo-L    0.0024   1.310    0.18    0.31    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 14:47:20 2001

Sample homogenised Area 2 Center #1

Refit _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _C -K' _O -K" 
Filter Fit Method
Chi-sqd = 2.19     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---        1346 +/-    44
  O -K       ---         ---         941 +/-    60
  Fe-L       ---         ---       10851 +/-   158
  Si-K    0.01696 +/- 0.00039       6965 +/-   160
  Mn-K    0.00688 +/- 0.00105        647 +/-    99
  Fe-K    0.97480 +/- 0.00613      80253 +/-   505
  Mo-L    0.00136 +/- 0.00067        323 +/-   159

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0167   1.527    4.96    2.55    +/- 0.06
  Mn-K    0.0068   1.025    0.69    0.70    +/- 0.11
  Fe-K    0.9613   1.005   94.25   96.57    +/- 0.61
  Mo-L    0.0013   1.312    0.10    0.18    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 14:49:36 2001

Sample homogenised Area 2 Center #2

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L" 
Filter Fit Method
Chi-sqd = 1.68     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         851 +/-    47
  O -K       ---         ---         438 +/-    63
  Fe-L       ---         ---       11113 +/-   137
  Si-K    0.01632 +/- 0.00045       6944 +/-   191
  Mn-K    0.00608 +/- 0.00113        591 +/-   110
  Fe-K    0.97563 +/- 0.00623      83194 +/-   531
  Mo-L    0.00197 +/- 0.00071        484 +/-   173

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0161   1.527    4.78    2.46    +/- 0.07
  Mn-K    0.0060   1.024    0.61    0.61    +/- 0.11
  Fe-K    0.9624   1.004   94.47   96.67    +/- 0.62
  Mo-L    0.0019   1.311    0.15    0.26    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 14:52:50 2001

Sample homogenised Area 2 Graphite #1

Refit _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _C -K' _Fe-L' _Mo-L  
Filter Fit Method
Chi-sqd = 1.88     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---        1665 +/-    55
  O -K       ---         ---        1499 +/-   126
  Fe-L       ---         ---       10991 +/-   196
  Si-K    0.01583 +/- 0.00047       6468 +/-   192
  Mn-K    0.00453 +/- 0.00116        423 +/-   108
  Fe-K    0.97964 +/- 0.00637      80223 +/-   522
  Mo-L    0.00000 +/- 0.00001          0 +/-     0

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0156   1.530    4.64    2.39    +/- 0.07
  Mn-K    0.0045   1.024    0.46    0.46    +/- 0.12
  Fe-K    0.9672   1.005   94.90   97.15    +/- 0.63
  Mo-L    0.0000   1.307    0.00    0.00    +/- 0.00
  Total                   100.00  100.00            




 

Thu Aug 16 14:55:28 2001

Sample homogenised Area 2 Graphite #2

Refit _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Si-K' 
Filter Fit Method
Chi-sqd = 1.59     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---        1419 +/-    63
  O -K       ---         ---         863 +/-   138
  Fe-L       ---         ---       11383 +/-   206
  Si-K    0.01715 +/- 0.00047       7150 +/-   197
  Mn-K    0.00647 +/- 0.00114        617 +/-   109
  Fe-K    0.97450 +/- 0.00629      81464 +/-   526
  Mo-L    0.00188 +/- 0.00074        452 +/-   178

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0169   1.527    5.01    2.58    +/- 0.07
  Mn-K    0.0064   1.025    0.65    0.65    +/- 0.12
  Fe-K    0.9607   1.005   94.20   96.52    +/- 0.62
  Mo-L    0.0019   1.312    0.14    0.24    +/- 0.10
  Total                   100.00  100.00            


Thu Aug 16 15:10:49 2001

As cast area #1 center analysis #1

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L' _Fe-L" 
Filter Fit Method
Chi-sqd = 1.89     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         757 +/-    46
  O -K       ---         ---         201 +/-    62
  Fe-L       ---         ---       12466 +/-   143
  Si-K    0.01647 +/- 0.00046       7129 +/-   198
  Mn-K    0.00630 +/- 0.00112        623 +/-   111
  Fe-K    0.97614 +/- 0.00625      84702 +/-   542
  Mo-L    0.00109 +/- 0.00072        273 +/-   179

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0162   1.528    4.82    2.48    +/- 0.07
  Mn-K    0.0062   1.025    0.63    0.64    +/- 0.11
  Fe-K    0.9630   1.005   94.47   96.74    +/- 0.62
  Mo-L    0.0011   1.311    0.08    0.14    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 15:13:21 2001

As cast area #1 center analysis #2

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L' 
Filter Fit Method
Chi-sqd = 2.48     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         764 +/-    45
  O -K       ---         ---         166 +/-    59
  Fe-L       ---         ---       11171 +/-   185
  Si-K    0.01581 +/- 0.00043       6872 +/-   189
  Mn-K    0.00357 +/- 0.00110        355 +/-   109
  Fe-K    0.97891 +/- 0.00622      85264 +/-   542
  Mo-L    0.00170 +/- 0.00070        426 +/-   176

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0156   1.528    4.64    2.39    +/- 0.07
  Mn-K    0.0035   1.024    0.36    0.36    +/- 0.11
  Fe-K    0.9661   1.004   94.88   97.03    +/- 0.62
  Mo-L    0.0017   1.311    0.13    0.22    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 15:15:47 2001

As cast area #1 center analysis #3

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Si-K' 
Filter Fit Method
Chi-sqd = 2.54     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         648 +/-    46
  O -K       ---         ---         220 +/-    64
  Fe-L       ---         ---       12607 +/-   195
  Si-K    0.01648 +/- 0.00045       7034 +/-   194
  Mn-K    0.00725 +/- 0.00111        707 +/-   108
  Fe-K    0.97614 +/- 0.00622      83495 +/-   532
  Mo-L    0.00013 +/- 0.00070         33 +/-   177

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0163   1.529    4.82    2.49    +/- 0.07
  Mn-K    0.0072   1.025    0.73    0.73    +/- 0.11
  Fe-K    0.9632   1.005   94.44   96.76    +/- 0.62
  Mo-L    0.0001   1.312    0.01    0.02    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 15:19:22 2001

As cast area #1 graphite analysis #1

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L" 
Filter Fit Method
Chi-sqd = 2.61     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         710 +/-    47
  O -K       ---         ---         232 +/-    65
  Fe-L       ---         ---       12963 +/-   148
  Si-K    0.01698 +/- 0.00046       7551 +/-   203
  Mn-K    0.00715 +/- 0.00109        728 +/-   111
  Fe-K    0.97521 +/- 0.00612      86935 +/-   546
  Mo-L    0.00066 +/- 0.00070        168 +/-   180

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0167   1.528    4.96    2.56    +/- 0.07
  Mn-K    0.0071   1.025    0.72    0.72    +/- 0.11
  Fe-K    0.9618   1.005   94.27   96.63    +/- 0.61
  Mo-L    0.0006   1.312    0.05    0.08    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 15:21:49 2001

As cast area #1 graphite analysis #2

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L" _Si-K' _Mo-L  
Filter Fit Method
Chi-sqd = 2.65     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         757 +/-    47
  O -K       ---         ---         170 +/-    65
  Fe-L       ---         ---       12843 +/-   147
  Si-K    0.01694 +/- 0.00046       7406 +/-   202
  Mn-K    0.00707 +/- 0.00109        706 +/-   109
  Fe-K    0.97600 +/- 0.00619      85527 +/-   542
  Mo-L    0.00000 +/- 0.00001          0 +/-     0

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0167   1.528    4.95    2.55    +/- 0.07
  Mn-K    0.0070   1.025    0.71    0.71    +/- 0.11
  Fe-K    0.9627   1.005   94.34   96.73    +/- 0.61
  Mo-L    0.0000   1.308    0.00    0.00    +/- 0.00
  Total                   100.00  100.00            




 

Thu Aug 16 15:28:42 2001

As cast area #2 center analysis #1

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L" 
Filter Fit Method
Chi-sqd = 2.60     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         650 +/-    46
  O -K       ---         ---         271 +/-    63
  Fe-L       ---         ---       13105 +/-   145
  Si-K    0.01615 +/- 0.00044       7087 +/-   194
  Mn-K    0.00359 +/- 0.00110        361 +/-   110
  Fe-K    0.97946 +/- 0.00614      86148 +/-   540
  Mo-L    0.00080 +/- 0.00070        202 +/-   177

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0159   1.529    4.73    2.44    +/- 0.07
  Mn-K    0.0035   1.025    0.36    0.36    +/- 0.11
  Fe-K    0.9666   1.005   94.85   97.10    +/- 0.61
  Mo-L    0.0008   1.311    0.06    0.10    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 15:31:09 2001

As cast area #2 center analysis #2

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L' _Fe-L" 
Filter Fit Method
Chi-sqd = 1.87     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         757 +/-    45
  O -K       ---         ---         168 +/-    60
  Fe-L       ---         ---       11985 +/-   140
  Si-K    0.01567 +/- 0.00044       6847 +/-   193
  Mn-K    0.00631 +/- 0.00113        630 +/-   113
  Fe-K    0.97578 +/- 0.00614      85443 +/-   538
  Mo-L    0.00223 +/- 0.00070        562 +/-   176

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0155   1.528    4.60    2.36    +/- 0.07
  Mn-K    0.0062   1.024    0.63    0.64    +/- 0.11
  Fe-K    0.9630   1.004   94.60   96.71    +/- 0.61
  Mo-L    0.0022   1.310    0.16    0.29    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 15:34:22 2001

As cast area #2 graphite analysis #1

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L" 
Filter Fit Method
Chi-sqd = 1.93     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         671 +/-    45
  O -K       ---         ---         170 +/-    63
  Fe-L       ---         ---       12668 +/-   144
  Si-K    0.01651 +/- 0.00046       7137 +/-   197
  Mn-K    0.00513 +/- 0.00111        508 +/-   110
  Fe-K    0.97823 +/- 0.00619      84752 +/-   536
  Mo-L    0.00012 +/- 0.00070         31 +/-   177

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0163   1.529    4.83    2.49    +/- 0.07
  Mn-K    0.0051   1.025    0.51    0.52    +/- 0.11
  Fe-K    0.9652   1.005   94.64   96.97    +/- 0.61
  Mo-L    0.0001   1.312    0.01    0.02    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 15:36:34 2001

As cast area #2 graphite analysis #2

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Filter Fit Method
Chi-sqd = 1.97     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         698 +/-    47
  O -K       ---         ---         113 +/-    64
  Fe-L       ---         ---       12529 +/-   196
  Si-K    0.01660 +/- 0.00045       7247 +/-   197
  Mn-K    0.00739 +/- 0.00110        737 +/-   110
  Fe-K    0.97496 +/- 0.00618      85301 +/-   541
  Mo-L    0.00105 +/- 0.00071        265 +/-   179

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0164   1.528    4.86    2.50    +/- 0.07
  Mn-K    0.0073   1.025    0.74    0.75    +/- 0.11
  Fe-K    0.9618   1.005   94.32   96.62    +/- 0.61
  Mo-L    0.0010   1.311    0.08    0.14    +/- 0.09
  Total                   100.00  100.00            


Thu Aug 16 15:42:55 2001

As cast area #3 center analysis #1

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Si-K' _Mo-L  
Filter Fit Method
Chi-sqd = 2.31     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         827 +/-    48
  O -K       ---         ---         257 +/-    65
  Fe-L       ---         ---       12122 +/-   195
  Si-K    0.01514 +/- 0.00045       6616 +/-   195
  Mn-K    0.00911 +/- 0.00112        910 +/-   112
  Fe-K    0.97575 +/- 0.00619      85460 +/-   542
  Mo-L    0.00000 +/- 0.00001          0 +/-     0

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0150   1.529    4.45    2.29    +/- 0.07
  Mn-K    0.0090   1.024    0.92    0.92    +/- 0.11
  Fe-K    0.9638   1.004   94.64   96.79    +/- 0.61
  Mo-L    0.0000   1.306    0.00    0.00    +/- 0.00
  Total                   100.00  100.00            




 

Thu Aug 16 15:45:08 2001

As cast area #3 center analysis #2

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Si-K" 
Filter Fit Method
Chi-sqd = 2.89     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         753 +/-    45
  O -K       ---         ---         242 +/-    64
  Fe-L       ---         ---       12129 +/-   196
  Si-K    0.01610 +/- 0.00028       6717 +/-   115
  Mn-K    0.00611 +/- 0.00111        583 +/-   106
  Fe-K    0.97557 +/- 0.00628      81562 +/-   525
  Mo-L    0.00223 +/- 0.00073        535 +/-   176

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0159   1.527    4.72    2.43    +/- 0.04
  Mn-K    0.0060   1.024    0.61    0.62    +/- 0.11
  Fe-K    0.9625   1.004   94.51   96.67    +/- 0.62
  Mo-L    0.0022   1.311    0.16    0.29    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 15:48:18 2001

As cast area #3 graphite analysis #1

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L' 
Filter Fit Method
Chi-sqd = 2.50     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         581 +/-    36
  O -K       ---         ---         196 +/-    50
  Fe-L       ---         ---       12093 +/-   159
  Si-K    0.01658 +/- 0.00037       7212 +/-   161
  Mn-K    0.00530 +/- 0.00100        527 +/-    99
  Fe-K    0.97574 +/- 0.00595      85067 +/-   519
  Mo-L    0.00237 +/- 0.00063        595 +/-   159

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0164   1.527    4.85    2.50    +/- 0.06
  Mn-K    0.0052   1.025    0.53    0.54    +/- 0.10
  Fe-K    0.9623   1.004   94.44   96.66    +/- 0.59
  Mo-L    0.0023   1.311    0.17    0.31    +/- 0.08
  Total                   100.00  100.00            




 

Thu Aug 16 15:50:23 2001

As cast area #3 graphite analysis #2

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L' _Fe-L" 
Filter Fit Method
Chi-sqd = 2.43     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         693 +/-    45
  O -K       ---         ---         226 +/-    60
  Fe-L       ---         ---       12686 +/-   142
  Si-K    0.01749 +/- 0.00045       7586 +/-   195
  Mn-K    0.00492 +/- 0.00111        488 +/-   110
  Fe-K    0.97714 +/- 0.00619      84955 +/-   538
  Mo-L    0.00045 +/- 0.00070        114 +/-   177

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0172   1.528    5.11    2.63    +/- 0.07
  Mn-K    0.0049   1.025    0.49    0.50    +/- 0.11
  Fe-K    0.9634   1.005   94.37   96.81    +/- 0.61
  Mo-L    0.0004   1.312    0.03    0.06    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 15:54:01 2001

As cast area 3 center analysis #3(area)

Refit _O -K' _O -K" 
Refit _Si-K" _Mn-K' _Mn-K" _Mo-L' 
Filter Fit Method
Chi-sqd = 2.91     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---        1572 +/-    55
  O -K       ---         ---         567 +/-    70
  Fe-L       ---         ---       10403 +/-   194
  Si-K    0.01096 +/- 0.00026       4514 +/-   106
  Mn-K    0.02009 +/- 0.00127       1892 +/-   120
  Fe-K    0.95812 +/- 0.00632      79092 +/-   522
  Mo-L    0.01083 +/- 0.00134       2569 +/-   317

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0108   1.523    3.25    1.65    +/- 0.04
  Mn-K    0.0199   1.022    2.04    2.03    +/- 0.13
  Fe-K    0.9475   1.002   93.91   94.92    +/- 0.63
  Mo-L    0.0107   1.302    0.80    1.39    +/- 0.17
  Total                   100.00  100.00            




 

Thu Aug 16 15:59:32 2001

As cast area3a center analysis #4(area)

Refit _O -K' _O -K" 
Refit _Si-K' _Mn-K' _Mn-K" _Mo-L" 
Filter Fit Method
Chi-sqd = 2.22     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---        1282 +/-    43
  O -K       ---         ---         433 +/-    57
  Fe-L       ---         ---       10846 +/-   158
  Si-K    0.01081 +/- 0.00035       4564 +/-   147
  Mn-K    0.01443 +/- 0.00112       1393 +/-   108
  Fe-K    0.96872 +/- 0.00603      81963 +/-   510
  Mo-L    0.00604 +/- 0.00069       1470 +/-   167

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0107   1.528    3.21    1.64    +/- 0.05
  Mn-K    0.0143   1.022    1.47    1.46    +/- 0.11
  Fe-K    0.9590   1.002   94.88   96.12    +/- 0.60
  Mo-L    0.0060   1.304    0.45    0.78    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 16:02:19 2001

As cast area3a graphite analys #1(area)

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Si-K' _Si-K" 
Filter Fit Method
Chi-sqd = 2.35     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         954 +/-    49
  O -K       ---         ---         349 +/-    66
  Fe-L       ---         ---       11776 +/-   194
  Si-K    0.01354 +/- 0.00026       5821 +/-   112
  Mn-K    0.01141 +/- 0.00115       1122 +/-   113
  Fe-K    0.97431 +/- 0.00618      83967 +/-   533
  Mo-L    0.00075 +/- 0.00072        185 +/-   179

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0134   1.530    3.99    2.05    +/- 0.04
  Mn-K    0.0113   1.024    1.15    1.15    +/- 0.12
  Fe-K    0.9635   1.004   94.80   96.70    +/- 0.61
  Mo-L    0.0007   1.309    0.06    0.10    +/- 0.09
  Total                   100.00  100.00            




 

Thu Aug 16 16:04:53 2001

As cast area3a graphite analys #2(area)

Refit _O -K' _O -K" _Mn-K' _Mn-K" _Mo-L' _Mo-L" 
Refit _Fe-L" _Si-K' 
Filter Fit Method
Chi-sqd = 2.12     Livetime = 60.0 Sec.   
Standardless Analysis
Element   Relative     Error        Net      Error
          k-ratio    (1-Sigma)     Counts  (1-Sigma)
  C -K       ---         ---         614 +/-    44
  O -K       ---         ---         192 +/-    63
  Fe-L       ---         ---       12895 +/-   145
  Si-K    0.01628 +/- 0.00044       7143 +/-   195
  Mn-K    0.00632 +/- 0.00111        635 +/-   111
  Fe-K    0.97716 +/- 0.00612      85919 +/-   538
  Mo-L    0.00024 +/- 0.00070         61 +/-   180

Adjustment Factors           K           L           M
  Z-Balance:             0.00000     0.00000     0.00000
  Shell:                 1.00000     1.00000     1.00000

PROZA Correction  Acc.Volt.= 15 kV  Take-off Angle=35.00 deg
Number of Iterations = 3

Element  k-ratio    ZAF   Atom %  Element  Wt % Err.
         (calc.)                    Wt %   (1-Sigma)
  Si-K    0.0161   1.529    4.77    2.46    +/- 0.07
  Mn-K    0.0062   1.025    0.63    0.64    +/- 0.11
  Fe-K    0.9643   1.005   94.58   96.87    +/- 0.61
  Mo-L    0.0002   1.312    0.02    0.03    +/- 0.09
  Total                   100.00  100.00            





